牛津仪器PMI-MASTER PRO
移动式直读光谱仪
鈥�技术参数
PMI-MASTER PRO移动式光谱仪用于固体样品元素定量分析的仪器。光学系统采用CCD检测器，光谱范围覆盖全部典型材料。
PMI-MASTER PRO移动式光谱仪技术参数
光学系统：
- Optical system 帕邢-龙格结构，
- Paschen – Runge Mount全息光栅 3000线/mm
- Focal length 350 mm焦距350 mm
- Detector system line detector with 2048 pixels 检测器系统：CCD检测器（每个CCD有2048像素）
- Pixel resolution 6 Pico meters像素分辨率 6 pm
- Reciprocal linear dispersion 0.9 nm/mm in 1st order色散率： 0,9 nm/mm （一级光谱）
- Wavelength coverage 170 – 420 nm波长范围： 170 – 420 nm
Sample Probes global探头基本描述
- JET STREAM-Function in case of Spark excitation in Argon atmosphere氩气喷射气流火花激发
- Optical signal at probe for Yes/No sorting 金属材料分选功能
- Pluggable pistol tube allowing fast exchange可插拔式设计便于快速切换
Standard Probe 标准探头
- Standard probe for arc and spark excitation, easily attachable to the main module 标准探头包含电弧和火花两种激发模式
- Standard cable – length 4 m (optional 8 m) 光纤标准长度 4m （选件可达8m）
- Equipped with HPC optical fibre 配备HPC光纤
- Ergonomically formed/shaped and balanced, probe weight ~ 800 g 探头设计精巧，重量800克
UVPRO 紫外探头
- Special sample probe for spark application, easy plugable to basic unit.用于火花应用的特殊激发枪，与主机易于连接，用于检测典型紫外元素(C, P, S, B, Sn, Se,As等)
- Wavelength coverage 170 – 200 nm, focal length 125mm, mechanically ruled grating with 3600 lines波长范围 170 – 200nm, 焦距 125mm, 机刻光栅 3600 线/mm
- Readout through CCD line detector with 3000 pixels, pixel resolution 6 pm读出系统： CCD-检测器（ 3000 像素）; 像素分辨率 6 pm
- Robust construction and compact design, integrated argon flushing system with short flush time of 2 – 3 minutes 坚固紧凑设计, 内置氩气冲洗装置，短冲洗时间（2-3分钟）
- Standard length 4 m (optional 8 m)光纤标准长度 4m （选件可达8m）
- Probe weight ~ 1200 g探头重量： 1200g
Source光源：
- Arc and spark excitation火花及电弧激发源
- Internally stabilized electronic control内置能量稳定器，电子调节
- Unipolar discharge单向放电
- Software controlled source parameter光源参数计算机控制
- Frequency: 110, 220 or 440 Hz频率： 110, 220 or 440 Hz
- Voltage: 35 450 V / Current: 1,5 – 3 A / Capacity: 2 µF, 3 µF / Inductivity: 80µH电压： 35 - 450 V / 电流： 1,5 – 3 A / 电容: 2 µF, 3 µF /电感: 80 µH
- HEPA Technology (Hepa Energy Pulsed Arc)高能脉冲电弧技术 (High Energy Pulsed Arc)
- Solid State Design固态振荡器设计
Computer & Readout system计算机及读出系统 (integrated hardware)
- Operating system Win7， Win7操作系统
- RAM > 2GB, 2 ¼” Notebook Hard Disc > 60 GB,
- Multi Channel A/D Converter多通道 A/D 转换
- Battery packed internal clock with real time and date function 电池供电实时时钟日期功能
- Interface：USB, PS2, Serial, VGA, LAN-Ethernet, Parallel配备接口, USB, PS2, 串口l, VGA, 局域网, 并口
Monitor显示屏
- Integrated high resolution 12” TFT-LCD monitor内置高清晰度12” 液晶显示器
- Scratch and break-proof industry Touch-screen坚固耐用工业触摸屏，无须键盘鼠标，易于操作
Software软件
- Operating system Win7； Win7 操作系统
- WAS lab Spectrometer software with following functions: WASlab 光谱仪软件，多任务操作：
- Material sorting原材料分选
- Unlimited programs for PMI tests多种PMI测试程序
- Selection of tolerance values and number of sparks for automatic calibration 自动根据给定偏差和激发次数进行标定控制
- Selection of number of sparks for PMI testing可选激发次数进行PMI测试
- Selectable counter for electrode cleaning根据设定数据进行电极清理
- Symetric and asymetric tolerances 对称及不对称偏差
- Element display and corresponding deviations during PMI testing PMI元素显示及相应偏差
- Storage and print option of measurement protocols检测结果存储及打印
- Free editable protocol header可自由编辑报告
- Grade quality detection牌号鉴别
- Data storage for more than 300 grade types per curve set每套曲线存储超过300个牌号数据
- Display of qualities during PMI testing PMI测试中显示牌号
- Quality ID via comparison of analytical values or quality search分析及搜索给出鉴定牌号
- Orientative analysis定向分析（成分近似分析）
- Unlimited amount of programs for orientative analysis分析程序无限制数量
- Display of raw intensities, intensity ratios, recalibrated and corrected intensity ratios
- 显示光强值、强度比、再校准和校正强度比
- Display of analyses in percent or ppm 分析结果百分含量或ppm显示
- 1- or 2-point recalibration1-2点曲线再校准
- Additive and multiplicative interelement correction相加和相乘的干扰校正
- Matrix correction基体校正
- Automatic line switch自动选择谱线
- Calculation of average values, standard deviation and variation coefficient for any number of burns任意激发次数的数据计算平均值、标准偏差及变异系数
- Marking of results which are beyond the calibration range结果超出曲线范围的标示
- Input sample identification样品标识输入
- Analytical data transfer to external PC possible分析数据可传输至外部计算机
- Connection of external printer and screen possible连接外部打印机及显示器
- Automatic hardware diagnostic硬盘故障自诊断
- Storage analytical values in standard format (Excel, ASCII, etc.) 分析数据以Excel, ASCII等标准格式存储
- Storage of complete spectral information for evaluation (optional)存储全谱信息用于评估（选件）
- Graphical display of spectra for qualitative evaluation (optional)用于牌号评估的光谱图显示（选件）
- Quick grade identification (FINGERPRINT)快速牌号鉴别（指纹技术）
- Storage capacity for more than 300 qualities per program每条曲线存储多于300个牌号
- Unlimited number of programs曲线数量无限制
- Matrix independent program layout
- Grade identification via spectral comparison of grades谱图对比鉴别牌号
TECHNICAL DATA 技术数据
Dimensions 尺寸:
- High高：196 mm, Depth长：512 mm, Width宽：470 mm,
- Weight重量：18 kg（不包含移动小车）
电源要求：
- 110/230 V 50/60 Hz
- Test Consumption 检测功率200 W
- Stand by Consumption待机功率50 W
- 16 A慢熔保险丝
氩气要求：
- 纯氩气, purity 5.0; 氩气减压阀regulator（5.0纯度氩气专配）99.999%;
- 气压5-6bar,Pressure min. 5 bar,max. 6 bar
- 塑料管传输r argon duct , unpolluted (e.g. solder)
PMI-MASTER PRO移动式光谱仪常见基体分析范围
|
铁基 |
|||||||||||||
|
序号 |
元素 |
Fe 100 |
Fe 200*** |
Fe 250*** |
Fe 300 |
Fe 400 |
Fe 500 |
||||||
|
低合金钢 |
铸铁 |
铬镍合金 |
不锈钢 |
工具钢 |
高锰钢 |
||||||||
|
下限% |
上限% |
下限% |
上限% |
下限% |
上限% |
下限% |
上限% |
下限% |
上限% |
下限% |
上限% |
||
|
1 |
C* |
0.003 |
1.6 |
- |
- |
- |
- |
0.003 |
2 |
0.005 |
2.6 |
0.005 |
1.7 |
|
2 |
Si |
0.005 |
2.25 |
0.025 |
3.6 |
0.025 |
7 |
0.02 |
4.5 |
0.005 |
1.5 |
0.005 |
1.5 |
|
3 |
Mn |
0.002 |
2.5 |
0.002 |
1.6 |
0.005 |
2.2 |
0.002 |
18 |
0.005 |
2 |
7 |
20 |
|
4 |
P* |
0.003 |
0.125 |
0.002 |
0.75 |
- |
- |
0.004 |
0.15 |
- |
- |
0.005 |
0.12 |
|
5 |
S* |
0.002 |
0.4 |
0.002 |
0.14 |
- |
- |
0.002 |
0.42 |
0.005 |
0.1 |
0.005 |
0.1 |
|
6 |
Ca* |
0.0001 |
0.001 |
- |
- |
- |
- |
- |
- |
- |
- |
- |
- |
|
7 |
Cr |
0.002 |
5.5 |
0.002 |
1.2 |
0.005 |
32 |
0.002 |
35 |
0.005 |
20 |
0.005 |
3.5 |
|
8 |
Mo |
0.003 |
1.8 |
0.005 |
1.5 |
0.005 |
3.5 |
0.005 |
6.5 |
0.005 |
11 |
0.005 |
1.8 |
|
9 |
Ni |
0.005 |
5.5 |
0.005 |
1.7 |
0.005 |
31 |
0.005 |
50 |
0.005 |
5 |
0.005 |
4.5 |
|
10 |
Al |
0.001 |
1.5 |
0.001 |
0.12 |
- |
- |
0.002 |
1.2 |
0.002 |
0.4 |
0.001 |
0.4 |
|
11 |
Co |
0.002 |
0.9 |
0.002 |
0.11 |
- |
- |
0.005 |
13 |
0.005 |
12 |
- |
- |
|
12 |
Cu |
0.002 |
0.8 |
0.002 |
1.6 |
0.002 |
8.5 |
0.001 |
6 |
0.001 |
1 |
0.002 |
0.25 |
|
13 |
Mg |
- |
- |
0.0005 |
0.1 |
- |
- |
- |
- |
- |
- |
- |
- |
|
14 |
Nb |
0.003 |
0.8 |
0.002 |
0.07 |
- |
- |
0.002 |
3.5 |
0.005 |
1 |
- |
- |
|
15 |
Ti |
0.001 |
0.5 |
0.001 |
0.33 |
- |
- |
0.002 |
2.5 |
0.002 |
0.5 |
- |
- |
|
16 |
V |
0.002 |
1 |
0.002 |
0.6 |
- |
- |
0.002 |
1 |
0.005 |
10 |
0.002 |
0.4 |
|
17 |
W |
0.02 |
2.25 |
- |
- |
- |
- |
0.02 |
4 |
0.04 |
22 |
- |
- |
|
18 |
Zr |
0.002 |
0.5 |
0.003 |
0.55 |
- |
- |
- |
- |
- |
- |
- |
- |
|
19 |
Sn* |
0.002 |
0.15 |
0.002 |
0.2 |
- |
- |
- |
- |
- |
- |
- |
- |
|
20 |
B* |
0.001 |
0.025 |
0.001 |
0.1 |
- |
- |
- |
- |
- |
- |
- |
- |
|
21 |
As* |
0.005 |
0.095 |
0.005 |
0.1 |
- |
- |
- |
- |
- |
- |
- |
- |
|
22 |
Bi* |
0.01 |
0.12 |
- |
- |
- |
- |
- |
- |
- |
- |
- |
- |
|
23 |
Pb |
0.01 |
0.35 |
0.01 |
0.25 |
- |
- |
- |
- |
- |
- |
- |
- |
|
24 |
Ce |
- |
- |
0.006 |
0.06 |
- |
- |
- |
- |
- |
- |
- |
- |
|
25 |
La |
- |
- |
0.002 |
0.022 |
- |
- |
- |
- |
- |
- |
- |
- |
|
26 |
Se* |
- |
- |
0.007 |
0.06 |
- |
- |
- |
- |
- |
- |
- |
- |
|
|
Fe |
内标元素 |
|||||||||||
注：*需配备UV紫外枪，***需配备专用火花枪
|
铝基 |
||||||
|
序号 |
元素 |
全范围分析曲线 |
||||
|
下限 % |
上限 % |
|||||
|
1 |
Si |
0,0020 |
25,00 |
|||
|
2 |
Fe |
0,0010 |
2,20 |
|||
|
3 |
Cu |
0,0020 |
8,00 |
|||
|
4 |
Mn |
0,0010 |
1,70 |
|||
|
5 |
Mg |
0,0001 |
12,00 |
|||
|
6 |
Cr |
0,0010 |
0,70 |
|||
|
7 |
Ni |
0,0050 |
3,20 |
|||
|
8 |
Zn |
0,0100 |
12,00 |
|||
|
9 |
Ti |
0,0010 |
0,30 |
|||
|
10 |
V |
0,0025 |
0,10 |
|||
|
11 |
Pb |
0,0050 |
1,60 |
|||
|
12 |
Ag |
0,0010 |
1,10 |
|||
|
13 |
B |
0,0010 |
0,025 |
|||
|
14 |
Be |
0,0010 |
0,015 |
|||
|
15 |
Bi |
0,0070 |
0,60 |
|||
|
16 |
Ca |
0,0010 |
0,020 |
|||
|
17 |
Ga |
0,0010 |
0,040 |
|||
|
18 |
Sn |
0,0050 |
0,35 |
|||
|
19 |
Sr |
0,0010 |
0,15 |
|||
|
20 |
Zr |
0,0020 |
0,25 |
|||
|
21 |
Cd |
0.0010 |
0,35 |
|||
|
22 |
Co |
0,0050 |
0,50 |
|||
|
23 |
Al |
内标元素 |
||||
|
No Standard Elements非标元素 |
|
|||||
|
24 |
In |
0,002 |
0,10 |
|||
|
铜基 |
|||||||
|
序号 |
元素 |
Cu U 000 |
Cu 000 |
Cu 100 |
|||
|
紫外枪程序 |
普通枪程序 |
子程序 |
|||||
|
|
|
下限 |
上限 |
下限 |
上限 |
下限 |
上限 |
|
1 |
Ag |
0.002 |
0.5 |
0.002 |
0.5 |
0.002 |
2 |
|
2 |
Al |
0.002 |
12 |
0.002 |
12 |
0.002 |
0.15 |
|
3 |
As |
0.003 |
0.5 |
0.015 |
0.5 |
- |
- |
|
4 |
Be |
0.002 |
0.6 |
0.002 |
0.6 |
0.002 |
2.6 |
|
5 |
Bi |
0.01 |
6 |
0.01 |
6 |
- |
- |
|
6 |
C |
0.002 |
0.03 |
0.002 |
0.03 |
- |
- |
|
7 |
Cd |
0.002 |
1.3 |
0.002 |
1.3 |
- |
- |
|
8 |
Co |
0.005 |
1 |
0.005 |
1 |
0.005 |
3.6 |
|
9 |
Cr |
0.002 |
2 |
0.002 |
2 |
0.002 |
0.1 |
|
10 |
Fe |
0.005 |
7 |
0.005 |
7 |
0.005 |
0.2 |
|
11 |
Mg |
0.005 |
0.2 |
0.005 |
0.2 |
- |
- |
|
12 |
Mn |
0.002 |
2 |
0.002 |
2 |
0.002 |
0.07 |
|
13 |
Ni |
0.01 |
37 |
0.01 |
37 |
0.005 |
0.12 |
|
14 |
P |
0.004 |
0.8 |
- |
- |
- |
- |
|
15 |
Pb |
0.015 |
22 |
0.015 |
22 |
- |
- |
|
16 |
S |
0.002 |
0.18 |
- |
- |
- |
- |
|
17 |
Sb |
0.01 |
0.6 |
0.01 |
0.6 |
- |
- |
|
18 |
Si |
0.005 |
8 |
0.005 |
8 |
0.005 | |
